Potassium Carbonate → 4-(2,6-Dichlorobenzyl)-2-(3,4-di methoxyphenyl)-2H-1,2,4-benzothiadiazin-3(4H)-one 1,1-dioxide

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Potassium Carbonate	HCID 11430	—
Edukt	2,6-Dichlorobenzyl chloride	HCID 74832	—
Edukt	2-(4-methoxy-3,5-dimethylphenyl)-4-(2,4,6-trifluorobenzyl)-2H-1,2,4-benzothiadiazin-3(4H)-one 1,1-dioxide	HCID 72722085	—
Lösungsmittel	Dimethylformamide	HCID 6228	—
Produkt	4-(2,6-Dichlorobenzyl)-2-(3,4-di methoxyphenyl)-2H-1,2,4-benzothiadiazin-3(4H)-one 1,1-dioxide	HCID 72721177	—

Reaktionsschritte

The title compound (52 mg, 0.11 mmol) was prepared from (IntA1) (67 mg, 0.20 mmol), K2CO3 (83 mg, 0.60 mmol) and 2,6-dichlorobenzyl chloride (47 mg, 0.24 mmol) in DMF (2 mL) using the methods of (115).

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US09249160B2
Quelldatensatz	uspto-grants-2016_02
ORD ID	ord-147a6dc193de46198f9533d273b59058
Quellennotiz	uspto-grants-2016_02