HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 90055164, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-chloro-1-ethylpiperidinium chloride | HCID 3084922 | — |
| Reactant | HCID 90055068 | HCID 90055068 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 90055164 | HCID 90055164 | — |
Reaction Steps
The title compound (42 mg, 0.09 mmol) was prepared from (IntE3) (100 mg, 0.31 mmol), 3-chloro-1-ethylpiperidine hydrochloride (142 mg, 0.77 mmol), KI (10.2 mg, 0.06 mmol) and K2CO3 (107 mg, 0.77 mmol) in DMF (5 mL) in a CEM Discover microwave reactor (100° C., 1 h) using the methods of (120).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09249160B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-3804313302cb478e8f11bd1e8a5b728b |
| Source note | uspto-grants-2016_02 |