HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 68586360, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-((1-Naphthalenyloxy)methyl)oxirane | HCID 91521 | — |
| Reactant | HCID 68587788 | HCID 68587788 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 68586360 | HCID 68586360 | — |
Reaction Steps
To a suspension of Compound 1 (0.17 g, 0.83 mmol) and Compound 2 (0.30 g, 0.83 mmol) in water (1 mL), triethylamine (0.10 g, 0.99 mmol) was added. The combined mixture was stirred at room temperature for 24 hours and then evaporated in the rotary evaporator to provide Compound 3 as a solid. This product was used without any workup and further purification. The structure of Compound 3 is given below:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09250249B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-f07f85d1785a4a11ba6d741fdea4311c |
| Source note | uspto-grants-2016_02 |