HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 71617090, compound → HCID 71617091, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 71617090 | HCID 71617090 | — |
| Solvent | tetrahydrofuran N,N-dimethylformamide | HCID 21974620 | — |
| Product | HCID 71617091 | HCID 71617091 | — |
Reaction Steps
Compound 12 (57 mg, 0.11 mmol) was dissolved in a mixture of DCM/TFA (1/1, 2 mL) and the reaction was stirred at RT for 6 h. The mixture was evaporated to dryness to recover compound 13 as a TFA salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09255095B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-e06db254140c4bd4831239bade9e84f0 |
| Source note | uspto-grants-2016_02 |