HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium carbonate → 4,6-bis(3,5-dimethylisoxazol-4-yl)-1H-benzo[d]imidazol-2(3H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 3,5-Dimethylisoxazole-4-boronic acid pinacol ester | HCID 2758656 | — |
| Reactant | HCID 86296389 | HCID 86296389 | — |
| Product | 4,6-bis(3,5-dimethylisoxazol-4-yl)-1H-benzo[d]imidazol-2(3H)-one | HCID 86296177 | — |
Reaction Steps
4,6-bis(3,5-dimethylisoxazol-4-yl)-1H-benzo[d]imidazol-2(3H)-one was synthesized using 3,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)isoxazole and Cs2CO3 in a similar fashion as 6-(3,5-dimethylisoxazol-4-yl)-4-(6-methylquinolin-5-yl)-1H-benzo[d]imidazol-2(3H)-one (Example 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09255089B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-046627fe002a4a69a23fff1c02c6294a |
| Source note | uspto-grants-2016_02 |