HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 117601993, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 117601220 | HCID 117601220 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 117601993 | HCID 117601993 | — |
Reaction Steps
3,5-Dicyclopropylisoxazole (70.0 mg, 0.469 mmol) was treated with NBS (167.0 mg, 0.938 mmol, equiv) in CH2Cl2 at room temperature for 12 h. The solvent was removed under a reduced pressure and the residue was directly loaded onto a silica gel column chromatography (hexane EtOAc 87:13) to give 4-bromo-3,5-dicyclopropylisoxazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09255089B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-c0fa978576e94d89a2bfb7ab4ff99d31 |
| Source note | uspto-grants-2016_02 |