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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1773726Generated: November 3, 2026

1,1'-Carbonyldiimidazole → HCID 86296966, compound

https://huagongshe.com/reaction/1773726

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,1'-CarbonyldiimidazoleHCID 68263—
ReactantHCID 117601099HCID 117601099—
SolventWaterHCID 962—
SolventTetrahydrofuranHCID 8028—
SolventEthyl AcetateHCID 8857—
ProductHCID 86296966HCID 86296966—

Reaction Steps

CDI (1.1 g, 6 mmol) was added to a solution of (2,3-diamino-5-(3,5-dimethylisoxazol-4-yl)phenyl)di(pyridin-2-yl)methanol (1.43 g, 3.7 mmol) in THF (10 mL) and the reaction mixture was stirred for 3 days. The reaction mixture was diluted with 100 mL water and 100 mL ethyl acetate and sonicated and filtered to yield the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09255089B2
Source datasetuspto-grants-2016_02
ORD IDord-206dc4a6b84749cba507317b2dfab6e6
Source noteuspto-grants-2016_02