HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1-Methylazetidin-3-yl)methanol → 2-iodo-4-(1-methylazetidin-3-ylmethoxy)-9,10-dihydro-4H-3,10a-diaza-benzo[f]azulene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1-Methylazetidin-3-yl)methanol | HCID 22967022 | — |
| Reactant | 4-Iodo-1-phenethyl-imidazole-2-carbaldehyde | HCID 86703945 | — |
| Product | 2-iodo-4-(1-methylazetidin-3-ylmethoxy)-9,10-dihydro-4H-3,10a-diaza-benzo[f]azulene | HCID 86703949 | — |
Reaction Steps
Compound 7A is obtained following the procedure already described in example 2A starting from compound 4-iodo-1-phenethyl-imidazole-2-carbaldehyde (example 2B) and (1-methylazetidin-3-yl)-methanol to give 2-iodo-4-(1-methylazetidin-3-ylmethoxy)-9,10-dihydro-4H-3,10a-diaza-benzo[f]azulene melting at 100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09255101B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-4741e9fe9eea497185a83d108b6e0499 |
| Source note | uspto-grants-2016_02 |