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HRID1773873

反应详情

EQUATION

反应方程式

HRID 1773873 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C(=O)O
HCID971

Oxalic acid

C2H2O4

结构：CN1CCC(OC2c3ccccc3CCn3cc(C=CC(=O)OC(C)(C)C)nc32)CC1
HCID86703959

未命名化合物

PRODUCTS

生成物

1
结构：CN1CCC(OC2c3ccccc3CCn3cc(C=CC(=O)OC(C)(C)C)nc32)CC1.O=C(O)C(=O)O
HCID131734714

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

3-[4-(1-methyl piperidin-4-yloxy)-9,10-dihydro-4H-3,10a-diaza-benzo[f]azulen-2-yl]-acrylic acid tert-butyl ester is dissolved in acetone (1.7 mL) and oxalic acid (1 equivalent) is added. Acetone is removed under reduced pressure to afford the compound as an oxalate.

WORKUP

后处理

  1. customAcetone is removed under reduced pressure