1-Bromopropane → HCID 178456332, compound

HRID 1774328Notes

Reaction equation

HRID 1774328 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[CH:11][N:10]=[CH:9]2)=[CH:4][CH:3]=1.Br[CH2:14][CH2:15][CH3:16]>C1COCC1>[Br-:1].[Br:1][C:2]1[CH:3]=[CH:4][C:5]([N+:8]2[CH:12]=[CH:11][N:10]([CH2:14][CH2:15][CH3:16])[CH:9]=2)=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 78401-BromopropaneHCID 27356041-(4-Bromophenyl)imidazole

Product 1

HCID 178456332HCID 178456332, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

According to the general synthesis procedure, 4.48 mmol (1.00 g) 1-(4-bromophenyl)imidazole and 5.40 mmol (0.660 g, 0.49 ml) 1-bromopropane are dissolved in 5 ml THF and heated for 20 h to 90° C.

Workup

  1. temperatureheated for 20 h to 90° C.

Sources & evidence

ORD record
ord-935666667ebb4e139a19f5b2d540c3ba
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

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