1-Bromoheptane → HCID 178443944, compound

HRID 1774330Notes

Reaction equation

HRID 1774330 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[CH:11][N:10]=[CH:9]2)=[CH:4][CH:3]=1.Br[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]>C1COCC1>[Br-:1].[Br:1][C:2]1[CH:3]=[CH:4][C:5]([N+:8]2[CH:12]=[CH:11][N:10]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])[CH:9]=2)=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 123691-BromoheptaneHCID 27356041-(4-Bromophenyl)imidazole

Product 1

HCID 178443944HCID 178443944, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

According to the general synthesis procedure, 1.62 mmol (0.361 g) 1-(4-bromophenyl)imidazole and 1.78 mmol (0.319 g, 0.28 ml) 1-bromoheptane are dissolved in 5 ml THF and heated for 2.5 h to 100° C.

Workup

  1. temperatureheated for 2.5 h to 100° C.

Sources & evidence

ORD record
ord-3bede0102ee645e5b834a6ca6a5edea1
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

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