HuagongsheHuagongshe Chemistry Print Report · For research reference only
Myristyl bromide → HCID 178443150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Myristyl bromide | HCID 8208 | — |
| Reactant | 1-(4-Bromophenyl)imidazole | HCID 2735604 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178443150 | HCID 178443150 | — |
Reaction Steps
According to the general synthesis procedure, 4.5 mmol (1.00 g) 1-(4-bromophenyl)imidazole and 5.4 mmol (1.50 g, 1.47 ml) 1-bromotetradecane are dissolved in 5 ml THF and heated for 69 h to 90° C. After the reaction the product is precipitated with diethylether from the reaction solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09260397B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-0713c9fb51fe4631b8aee4db3b53bbb1 |
| Source note | uspto-grants-2016_02 |