HuagongsheHuagongshe Chemistry Print Report · For research reference only
Myristyl bromide → 1-(4-Chlorophenyl)-3-tetradecyl imidazolium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Myristyl bromide | HCID 8208 | — |
| Reactant | 1-(4-Chlorophenyl)-1H-imidazole | HCID 142859 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1-(4-Chlorophenyl)-3-tetradecyl imidazolium bromide | HCID 178443152 | — |
Reaction Steps
According to the general synthesis procedure 5.6 mmol (1.00 g) 1-(4-chlorophenyl)imidazole and 6.7 mmol (1.86 g, 1.82 ml) 1-bromotetradecane are dissolved in 5 ml THF and heated for 42 h to 90° C. At the end of the reaction the reaction mixture is cooled down to room temperature and the product is precipitated with diethylether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09260397B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-102dde7402434d619b8f589ac226a8b0 |
| Source note | uspto-grants-2016_02 |