HuagongsheHuagongshe Chemistry Print Report · For research reference only
Myristyl bromide → HCID 178443153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Myristyl bromide | HCID 8208 | — |
| Reactant | 1-(4-Nitrophenyl)-1H-imidazole | HCID 123155 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178443153 | HCID 178443153 | — |
Reaction Steps
According to the general synthesis procedure, 5.3 mmol (1.00 g) 1-(4-nitrophenyl)imidazole and 6.3 mmol (1.76 g, 1.70 ml) 1-bromotetradecane are dissolved in 5 ml THF and heated for 45 h to 90° C. At the end of the reaction the reaction mixture is cooled down to room temperature and the precipitated product is washed with THF and diethylether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09260397B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-fb10579894f846b9b14e4c296bb1a03a |
| Source note | uspto-grants-2016_02 |