1-Bromopropane → HCID 178462651, compound

HRID 1774343Notes

Reaction equation

HRID 1774343 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]([CH3:12])[CH3:11])[C:5]=1[N:13]1[CH:17]=[CH:16][N:15]=[CH:14]1)([CH3:3])[CH3:2].[Br:18][CH2:19][CH2:20]C>C1COCC1>[Br-:18].[CH:1]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]([CH3:12])[CH3:11])[C:5]=1[N+:13]1[CH:17]=[CH:16][N:15]([CH2:19][CH3:20])[CH:14]=1)([CH3:2])[CH3:3]

Participants

4

Reactant 2

HCID 78401-BromopropaneHCID 158792651-(2,6-diisopropylphenyl)-1H-imidazole

Product 1

HCID 178462651HCID 178462651, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

According to the general synthesis procedure, 4.4 mmol (1.00 g) 1-(2,6-diisopropylphenyl)imidazole and 5.3 mmol (0.650 g, 0.48 ml) 1-bromopropane are dissolved in 5 ml THF and heated for 20 h to 90° C.

Workup

  1. temperatureheated for 20 h to 90° C.

Sources & evidence

ORD record
ord-92b85a1758664ccc880edfd0450e9550
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

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