1-Bromoheptane → HCID 178444694, compound

HRID 1774344Notes

Reaction equation

HRID 1774344 reaction equation
[CH:1]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]([CH3:12])[CH3:11])[C:5]=1[N:13]1[CH:17]=[CH:16][N:15]=[CH:14]1)([CH3:3])[CH3:2].[Br:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24]C>C1COCC1>[Br-:18].[CH:1]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([CH:10]([CH3:12])[CH3:11])[C:5]=1[N+:13]1[CH:17]=[CH:16][N:15]([CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])[CH:14]=1)([CH3:2])[CH3:3]

Participants

4

Reactant 2

HCID 123691-BromoheptaneHCID 158792651-(2,6-diisopropylphenyl)-1H-imidazole

Product 1

HCID 178444694HCID 178444694, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

According to the general synthesis procedure 4.4 mmol (1.00 g) 1-(2,6-diisopropylphenyl)imidazole and 5.3 mmol (0.940 g, 0.83 ml) 1-bromoheptane are dissolved in 5 ml THF and heated for 20 h to 110° C.

Workup

  1. temperatureheated for 20 h to 110° C.

Sources & evidence

ORD record
ord-73c0f157cc8746109aa98ec06ec48d68
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

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