1-Bromopropane → HCID 178456335, compound

HRID 1774346Notes

Reaction equation

HRID 1774346 reaction equation
[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[N:10]1[CH:14]=[CH:13][N:12]=[CH:11]1)[CH3:2].[Br:15][CH2:16][CH2:17][CH3:18]>C1COCC1>[Br-:15].[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[N+:10]1[CH:14]=[CH:13][N:12]([CH2:16][CH2:17][CH3:18])[CH:11]=1)[CH3:2]

Participants

4

Reactant 2

HCID 78401-BromopropaneHCID 58249724HCID 58249724, compound

Product 1

HCID 178456335HCID 178456335, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

According to the general synthesis procedure, 5.3 mmol (1.00 g) 1-(2-ethoxyphenyl)imidazole and 6.4 mmol (0.780 g, 0.58 ml) 1-bromopropane are dissolved in 5 ml THF and heated for 21 h to 90° C.

Workup

  1. temperatureheated for 21 h to 90° C.

Sources & evidence

ORD record
ord-34d8ffade2ae48e0bd3702a3f4b3dfba
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

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