1-Bromohexane → HCID 178444695, compound

HRID 1774351Notes

Reaction equation

HRID 1774351 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([N:9]2[CH:13]=[CH:12][N:11]=[CH:10]2)=[CH:5][CH:4]=1.[Br:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]>C1COCC1>[Br-:14].[CH2:15]([N:11]1[CH:12]=[CH:13][N+:9]([C:6]2[CH:7]=[CH:8][C:3]([O:2][CH3:1])=[CH:4][CH:5]=2)=[CH:10]1)[CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]

Participants

4

Reactant 2

HCID 81011-BromohexaneHCID 823281-(4-Methoxyphenyl)imidazole

Product 1

HCID 178444695HCID 178444695, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

According to the general synthesis procedure, 10.40 mmol (1,812 g) 1-(4-methoxyphenyl)imidazole and 11.44 mmol (1,889 g, 1.65 ml) 1-bromohexane are dissolved in 5 ml THF and heated for 12 h to 80° C.

Workup

  1. temperatureheated for 12 h to 80° C.

Sources & evidence

ORD record
ord-acdab5281f8a433ea4ced7d95167f922
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

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