1-Bromoheptane → HCID 178443952, compound

HRID 1774352Notes

Reaction equation

HRID 1774352 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([N:9]2[CH:13]=[CH:12][N:11]=[CH:10]2)=[CH:5][CH:4]=1.[Br:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]>C1COCC1>[Br-:14].[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([N+:9]2[CH:13]=[CH:12][N:11]([CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])[CH:10]=2)=[CH:5][CH:4]=1

Participants

4

Reactant 2

HCID 123691-BromoheptaneHCID 823281-(4-Methoxyphenyl)imidazole

Product 1

HCID 178443952HCID 178443952, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

According to the general synthesis procedure 5.7 mmol (1.00 g) 1-(4-methoxyphenyl)imidazole and 6.9 mmol (1.23 g, 1.1 ml) 1-bromoheptane are dissolved in 5 ml THF and heated for 18 h to 90° C.

Workup

  1. temperatureheated for 18 h to 90° C.

Sources & evidence

ORD record
ord-3eee689701a84108a9fd784733cdda96
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

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