1-Bromohexane → HCID 178444691, compound

HRID 1774353Notes

Reaction equation

HRID 1774353 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[N:9]1[CH:13]=[CH:12][N:11]=[CH:10]1.[Br:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]>C1COCC1>[Br-:14].[CH2:15]([N:11]1[CH:12]=[CH:13][N+:9]([C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[O:2][CH3:1])=[CH:10]1)[CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]

Participants

4

Reactant 2

HCID 81011-BromohexaneHCID 5305516HCID 5305516, compound

Product 1

HCID 178444691HCID 178444691, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

According to the general synthesis procedure, 10.40 mmol (1,812 g) 1-(2-methoxyphenyl)imidazole and 11.44 mmol (1,889 g, 1.65 ml) 1-bromohexane are dissolved in 5 ml THF and heated for 5 h to 80° C.

Workup

  1. temperatureheated for 5 h to 80° C.

Sources & evidence

ORD record
ord-ed90b8318ca14ab3a2590fe9cda72f83
Source dataset
uspto-grants-2016_02
Patent number
US09260397B2

Reaction notes

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