HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 86679130, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Reactant | 6-bromo-7-fluoro-3,4-dihydroquinolin-2(1H)-one | HCID 43457689 | — |
| Product | HCID 86679130 | HCID 86679130 | — |
Reaction Steps
In analogy to the procedure described for the preparation of intermediates A-1 [A], 6-bromo-7-fluoro-3,4-dihydro-1H-quinolin-2-one was reacted with methyl iodide in presence of potassium tert-butoxide to give the title compound as a white foam. MS: 258.0, 259.9 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09260408B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-549ee427621a4463b9d21615c0191f7a |
| Source note | uspto-grants-2016_02 |