HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 89440221, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 89440465 | HCID 89440465 | — |
| Product | HCID 89440221 | HCID 89440221 | — |
Reaction Steps
In analogy to the procedure described for the preparation of intermediate A-41, N-(1-(5-bromopyridin-3-yl)ethyl)ethanesulfonamide (intermediate A-37) was reacted with MeI in presence of NaH (60% in mineral oil) to give the title compound as a light yellow solid. MS: 307.1 and 309.2 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09260408B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-036b67e7001b4342ac539ac4e1e705c5 |
| Source note | uspto-grants-2016_02 |