HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium trimethylsilanolate → HCID 86679168, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium trimethylsilanolate | HCID 23668039 | — |
| Reactant | HCID 59619900 | HCID 59619900 | — |
| Product | HCID 86679168 | HCID 86679168 | — |
Reaction Steps
In analogy to the procedure described for the preparation of example 59 [B], methyl 2-(5-bromopyridin-3-yl)-2-methylpropanoate (example 72 [A]) was reacted with 90% potassium trimethylsilanolate to give the title compound as a light brown solid. MS: 244.3 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09260408B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-4007e43126304e8aaf282e05f54ca073 |
| Source note | uspto-grants-2016_02 |