HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 118034959, compound → 1206978-90-6
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 118034959 | HCID 118034959 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1206978-90-6 | HCID 68294747 | 100.4% |
Reaction Steps
A mixture of 1.82 g of 7-bromo-2-trifluoromethyl-2,3-dihydroimidazo[1,2-a]pyridin-2-ol hydrobromide and 10 ml of ethanol was stirred under heat-reflux for 1 day. The cooled reaction mixture was concentrated under reduced pressure, then water was added, and the mixture was extracted with ethyl acetate. The mixture was dried over anhydrous sodium sulfate and concentrated under reduced pressure to obtain 1.33 g of 7-bromo-2-trifluoromethylimidazo[1,2-a]pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09260436B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-98065be5b3884d4b8ad934316287c4f4 |
| Source note | uspto-grants-2016_02 |