HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 102189385, compound → HCID 87145216, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 102189385 | HCID 102189385 | — |
| Reactant | HCID 131734742 | HCID 131734742 | — |
| Product | HCID 87145216 | HCID 87145216 | 85% |
Reaction Steps
Except that 3-(phenylsulfenyl)-2-iodobenzo[b]thiophene was replaced with 3-(phenylselenenyl)-2-iodobenzo[b]thiophene, the reaction was implemented in the same way as in Example 3. Purification was implemented by column chromatography (silica gel, CHCl3, Rf: 0.9), so that a yellow solid was produced (yield: 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09260451B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-1c0158f47b434c0ebc840590c79f3e43 |
| Source note | uspto-grants-2016_02 |