HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Iodobenzaldehyde → HCID 66576644, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Iodobenzaldehyde | HCID 252610 | — |
| Reactant | HCID 66576809 | HCID 66576809 | — |
| Product | HCID 66576644 | HCID 66576644 | — |
Reaction Steps
Compound 3 was synthesised following similar procedures outlined in Example 25 (Compound 20), using 3-iodobenzaldehyde instead of 2-methylbenzaldehyde in Step 1. As a slightly modified procedure, the crude residue of Step 3 was purified by column chromatography (silica gel, gradient 80 to 100% CH2Cl2/isohexane to 2% diethyl ether/CH2Cl2), yielding Compound 3 as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09260381B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-33038571ffe444f69addacdad927ee9e |
| Source note | uspto-grants-2016_02 |