HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Furanol, tetrahydro- → HCID 66576410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Furanol, tetrahydro- | HCID 9960 | — |
| Reactant | CID 86697018 | HCID 86697018 | — |
| Product | HCID 66576410 | HCID 66576410 | 34.8% |
Reaction Steps
Compound 97 was synthesised from 4-chloro-3,5-diphenyl-1H-pyrazolo[3,4-c]pyridazine (50 mg, 0.16 mmol) following a similar procedure outlined in Example 86, using 3-hydroxytetrahydrofuran (28 mg, 0.32 mmol) instead of oxetan-3-ol. Compound 97 was purified using preparative HPLC followed by chromatography (silica gel, gradient CH2Cl2), yielding Compound 97 as an off-white solid (21 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09260381B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-e3ca3b6b650e4bd8a76ec614ffba1fb3 |
| Source note | uspto-grants-2016_02 |