HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl trifluoroacetate → HCID 89653236, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl trifluoroacetate | HCID 9794 | — |
| Reactant | HCID 117774129 | HCID 117774129 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 89653236 | HCID 89653236 | — |
Reaction Steps
A solution of 800 mg of 19-phenyl-3,6,9,12,15,18-hexaoxanonadecylammonium acetate in 5 ml of MeOH was admixed with 75 μl of TEA and 609 μl of ethyl trifluoroacetate, and stirred at RT for 17 h. Solvents and excess reagents were removed, and the residue was filtered on a silica gel column (EE). Yield: 672 mg of colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09260467B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-56992a10db96414496adb1554a64eab9 |
| Source note | uspto-grants-2016_02 |