Hydrochloric Acid → HCID 89653161, compound

Participants

Reaction Steps

672 mg of compound 14 were dissolved in 5 ml of MeOH, and the solution was adjusted to a pH of 3 with HCl and, following addition of 76 mg of Pd on carbon (10%), was hydrogenated under atmospheric pressure for 17 h. The suspension was filtered over Celite, concentrated, and coevaporated twice with toluene. Solvent residues were removed overnight under an oil pump vacuum. Yield: 480 mg of colourless oil.

Provenance & Evidence