HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86679495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 71543203 | HCID 71543203 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86679495 | HCID 86679495 | 125.9% |
Reaction Steps
(S)-3,5-dichloro-4-(2-(3-(cyclopropylmethoxy)-4-(difluoromethoxy)phenyl)-2-(2-(4-methoxy-3-(N-(2-morpholinoethyl)methylsulfonamido)benzoyloxy)-acetoxy)ethyl)pyridine 1-oxide (21 mg, 0.026 mmol) was dissolved in EtOAc (1 ml). HCl 2M in Et2O (15 μl) was added, then Et2O (5 ml) was added. The precipitate was filtered and dried in the vacuum oven to give 14 mg of final product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09265768B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-b3ce2463c6a541078ab069faec2ec453 |
| Source note | uspto-grants-2016_02 |