HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 31699716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 3-(4-Methyl-1-piperazinylsulfonyl)benzoic Acid | HCID 1081456 | — |
| Product | HCID 31699716 | HCID 31699716 | — |
Reaction Steps
3-((4-methylpiperazin-1-yl)sulfonyl)benzoic acid (250 mg, 0.879 mmol) was refluxed in the presence of concentrated sulfuric acid (5.68 mg, 0.044 mmol) in methanol at 70° C. for overnight. Reaction was monitored by TLC. After completion of the reaction, solvent was removed by vacuum and the crude material was used for further reaction without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266838B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-bae0fabb4ea647a8845097414d1ade20 |
| Source note | uspto-grants-2016_02 |