HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-1-propanol → HCID 118201023, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-1-propanol | HCID 9086 | — |
| Reactant | Ethyl oxoacetate | HCID 70211 | — |
| Reactant | 5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoic acid | HCID 53260165 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 118201023 | HCID 118201023 | — |
Reaction Steps
By using ethyl glyoxylate (polymer type, a solution of 47% toluene) (4.3 mL, 20.4 mol), 3-aminopropan-1-ol (1.6 mL, 20.4 mmol) and 5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoic acid (1.0 g, 4.9 mmol), the same procedure as in Reference Example 1 was carried out to obtain the title compound (1.3 g) (colorless solid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266870B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-17c557de0355419e8f818c38449ea325 |
| Source note | uspto-grants-2016_02 |