HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl oxoacetate → HCID 118020502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl oxoacetate | HCID 70211 | — |
| Reactant | 3-amino-2-methylpropan-1-ol | HCID 10197625 | — |
| Reactant | 5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoic acid | HCID 53260165 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 118020502 | HCID 118020502 | — |
Reaction Steps
By using 3-amino-2-methylpropan-1-ol (0.10 g, 1.1 mmol), ethyl glyoxylate (polymer type, a solution of 47% toluene) (2.0 mL, 9.7 mmol) and 5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoic acid (0.5 g, 2.5 mmol), the same procedure as in Reference Example 1 was carried out to obtain the title compound (0.13 g) (colorless oil).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266870B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-4fb2f892bb1f48e5863fb6756a515198 |
| Source note | uspto-grants-2016_02 |