HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 10406441, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | N-[3,5-bis(trifluoromethyl)phenyl]-2-hydroxy-5-nitro-benzamide | HCID 11741321 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 10406441 | HCID 10406441 | — |
Reaction Steps
N-(3,5-bis-trifluoromethyl-phenyl)-2-hydroxy-5-nitro-benzamide (400 mg, 1.4 mmol) prepared in step 1 was dissolved in 4.2 . of isopropanol (IPA), to which 3 g of iron powder and 3 . of NH4Cl saturated solution were added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266872B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-e35eed8f7f2748c9a78cee72ca3d21d3 |
| Source note | uspto-grants-2016_02 |