HuagongsheHuagongshe Chemistry Print Report · For research reference only
benzyl 2-(4-((dimethylamino)methyl)-3,5-dimethyl-1H-pyrazol-1-yl)acetate → benzyl 2-(3,5-dimethyl-1H-pyrazol-1-yl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | benzyl 2-(4-((dimethylamino)methyl)-3,5-dimethyl-1H-pyrazol-1-yl)acetate | HCID 89726461 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | benzyl 2-(3,5-dimethyl-1H-pyrazol-1-yl)acetate | HCID 52463841 | — |
Reaction Steps
The final compound was prepared using a method analogous to that of Example 14 step 14.2, benzyl 2-(4-((dimethylamino)methyl)-3,5-dimethyl-1H-pyrazol-1-yl)acetate replacing intermediate 14.1 and using EtOH instead of MeOH/AcOH. LC-MS (B): tR=0.23 min; [M+H]+: 212.17.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266876B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-a63e5f18b17b4fbb88c9008d94eef1ee |
| Source note | uspto-grants-2016_02 |