HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutanol → HCID 118036774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutanol | HCID 6560 | — |
| Reactant | 6-Amino-4-fluoronicotinonitrile | HCID 118036901 | — |
| Product | HCID 118036774 | HCID 118036774 | — |
Reaction Steps
From intermediate 21 and 2-methylpropan-1-ol, reacted in an analogous manner to the preparation of intermediate 89. 1H NMR (400 MHz, DMSO-d6) δ 8.13 (s, 1H), 7.86 (s, br, 2H), 6.04 (s, 1H), 3.79 (d, 2H), 2.06-1.96 (m, 1H), 0.96 (d, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266883B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-46a545715578426aaeb73bbadec95fcd |
| Source note | uspto-grants-2016_02 |