HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethylamine → 5-Bromo-2-(2-methoxyethyl)isoindolin-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethylamine | HCID 8018 | — |
| Reactant | 4-Bromo-2-(bromomethyl)benzoate | HCID 23158145 | — |
| Product | 5-Bromo-2-(2-methoxyethyl)isoindolin-1-one | HCID 59276302 | — |
Reaction Steps
This compound was prepared by using procedures analogous to those described for the synthesis of Example 52, Step 6 starting from 4-bromo-2-(bromomethyl)benzoate (AstaTech Cat. No. 27012) and 2-methoxyethylamine (Aldrich Cat No. 241067). LCMS (M+H)+=270.0/272.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266892B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-b4525711ad4e48e8bb17c63b63fe4a39 |
| Source note | uspto-grants-2016_02 |