HCID 4305401, compound → HCID 10261979, compound

Participants

Reaction Steps

To a solution of EXAMPLE 65A (2.36 g) in toluene (30 mL) was added diisobutylaluminum hydride (1.5M in toluene, 8 mL) at −78° C. After stirring for 10 minutes the reaction mixture was quenched by addition of water. The precipitate was removed by filtration through diatomaceous earth. The filtrate was washed with water and brine and dried over Na2SO4. Filtration and evaporation of solvent provided the title compound.

Provenance & Evidence