HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 89498001, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 89498369 | HCID 89498369 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 89498001 | HCID 89498001 | — |
Reaction Steps
A solution of EXAMPLE 77B (0.34 g) and hydrochloric acid (2 mL) in tetrahydrofuran (3.5 mL) was stirred at room temperature for 16 hours. The reaction mixture was concentrated, redissolved in dichloromethane, dried over magnesium sulfate, filtered, and used in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266877B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-9d9b962fcfc2432b8fa725e31fb559fb |
| Source note | uspto-grants-2016_02 |