HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89498195, compound → HCID 118106884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89498195 | HCID 89498195 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 118106884 | HCID 118106884 | — |
Reaction Steps
A mixture of EXAMPLE 186A (6.5 g) and formic acid (20 mL) was heated at 100° C. for 3 hours. The reaction mixture was concentrated, and the residue was purified by silica gel chromatography, eluting with 1% ethyl acetate in petroleum ether, to give the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09266877B2 |
| Source dataset | uspto-grants-2016_02 |
| ORD ID | ord-ad6a274bace74fb3b56c7c03287857f6 |
| Source note | uspto-grants-2016_02 |