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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1778937Generated: November 3, 2026

HCID 89498195, compound → HCID 118106884, compound

https://huagongshe.com/reaction/1778937

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 89498195HCID 89498195—
SolventFormic AcidHCID 284—
ProductHCID 118106884HCID 118106884—

Reaction Steps

A mixture of EXAMPLE 186A (6.5 g) and formic acid (20 mL) was heated at 100° C. for 3 hours. The reaction mixture was concentrated, and the residue was purified by silica gel chromatography, eluting with 1% ethyl acetate in petroleum ether, to give the title product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09266877B2
Source datasetuspto-grants-2016_02
ORD IDord-ad6a274bace74fb3b56c7c03287857f6
Source noteuspto-grants-2016_02