Sulfuric Acid → 407610-92-8

HRID 1779139Notes

Reaction equation

HRID 1779139 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]2[C:7](=[CH:8][CH:9]=1)[C:6](Br)(Br)[CH2:5]2.S(=O)(=O)(O)[OH:13]>O>[Br:1][C:2]1[CH:3]=[C:4]2[C:7](=[CH:8][CH:9]=1)[C:6](=[O:13])[CH2:5]2

Participants

4

Reactant 2

HCID 1118Sulfuric AcidHCID 71187153HCID 71187153, compound

Product 1

HCID 15547951407610-92-8

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
75 °C

Procedure

To a suspension of 3-bromo-7,7-dibromo-bicyclo[4.2.0]octa-1,3,5-triene (2) (186.2 g, 0.546 mol, theoretical) in H2O (1000 ml) was added sulfuric acid (97%, 50 ml) at 15° C. The resulting mixture was stirred at 75° C. for 4.5 days.

Sources & evidence

ORD record
ord-d8d75b99a9574cfb9bee464bc44e6d4e
Source dataset
uspto-grants-2016_02
Patent number
US09269927B2

Reaction notes

Loading…