Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 71187153 | HCID 71187153 | — |
| Solvent | Water | HCID 962 | — |
| Product | 407610-92-8 | HCID 15547951 | — |
Reaction Steps
To a suspension of 3-bromo-7,7-dibromo-bicyclo[4.2.0]octa-1,3,5-triene (2) (186.2 g, 0.546 mol, theoretical) in H2O (1000 ml) was added sulfuric acid (97%, 50 ml) at 15° C. The resulting mixture was stirred at 75° C. for 4.5 days.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09269927B2 |
|---|
| Source dataset | uspto-grants-2016_02 |
|---|
| ORD ID | ord-d8d75b99a9574cfb9bee464bc44e6d4e |
|---|
| Source note | uspto-grants-2016_02 |
|---|
