Hydrochloric Acid → HCID 19956421, compound

Participants

Reaction Steps

A mixture of 0.55 g (0.805 mmol) of (E)-1-allyl-14-propyl-1,5,10,14-tetra-BOC-1,5,10,14-tetraazatetradec-7-ene and 8.2 ml of 3N methanolic hydrochloric acid is reacted analogously to Example 8. The resulting title compound melts at >260° C. 1H-NMR (D2O): δ0.97(t,3H); 1.63-1.76(m,2H); 2.05-2.16(m,4H); 3.02(t,2H); 3.11-3.19(m,8H); 3.69(d,2H); 3.77(d,4H); 5.48-5.55(m,2H); 5.83-5.98(m,1H); 6.04-6.07(m,2H).

Provenance & Evidence