Hydrochloric Acid → HCID 19956423, compound

Participants

Reaction Steps

A mixture of 0.6 g (0,916 mmol) of (E)-1-allyl-14-methyl-1,5,10,14-tetra-BOC-1,5,10,14-tetraazatetradec-7-ene and 9 ml of 3N methanolic hydrochloric acid is reacted analogously to Example 8. The resulting title compound melts at >260° C. 1H-NMR (D2O): δ2.07-2.17(m,4H); 2.73(s,3H); 3.12-3.19(m,8H); 3.69(d,2H); 3.77(d,4H); 5.48-5.55(m,2H); 5.83-5.98(m, 1H); 6.04-6.07 (m,2H).

Provenance & Evidence