HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trichloroacetic Acid → HCID 54097936, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trichloroacetic Acid | HCID 6421 | — |
| Reactant | HCID 86750802 | HCID 86750802 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54097936 | HCID 54097936 | — |
Reaction Steps
Using the procedure described in J. Chem. Soc., 1956, 4330, (3β,5α,11β,12β,25R)-23-bromo-11,12-epoxyspirostan-3-ol was treated with trichloroacetic acid in toluene at room temperature for 3 days to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05629295 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-bb0af9c4b769443fbc6377d7ccbe1886 |
| Source note | uspto-grants-1997_05 |