HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 54124296, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 14737528 | HCID 14737528 | — |
| Product | HCID 54124296 | HCID 54124296 | — |
Reaction Steps
Under cooling, 1.8 ml of thionyl chloride was dropwise added slowly to 20 ml of methanol. After 10 minutes, 1.5 g of 7-methoxy-1-oxo-1,2,3,4-tetrahydronaphthalene-2-acetic acid was added and stirred overnight at room temperature. The solvent was distilled off under reduced pressure to obtain 1.6 g of methyl 7-methoxy-1-oxo-1,2,3,4-tetrahydronaphthalene-2-acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05629321 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-607ab643cafe42449ff68db610af9941 |
| Source note | uspto-grants-1997_05 |