Water → HCID 178507419, compound

Participants

Reaction Steps

A 5 g portion of 4-triazolylnitrobenzene dissolved in 20 ml of acetic acid was mixed with 0.3 g of 10% Pd-carbon and subjected to hydrogenation under a hydrogen pressure of 3 kg/cm2. The reaction solution was poured into water and extracted with chloroform. The resulting organic layer was washed with sodium bicarbonate aqueous solution and water in that order and dried, and the solvent was removed by evaporation under a reduced pressure to obtain 3 g of 4-triazolylaniline with a yield of 71%.

Provenance & Evidence