Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Diosmetin | HCID 5281612 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 9910029 | HCID 9910029 | — |
Reaction Steps
30 g of diosmetin in 300 ml of dimethylformamide are added to a suspension of 11.7 g of sodium hydride in 150 ml of dimethylformamide. The mixture is maintained at 40° C. with stirring until the evolution of gas has ceased. 48 g of allyl bromide are then added and stirring at 40° C. is continued for 22 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05629339 |
|---|
| Source dataset | uspto-grants-1997_05 |
|---|
| ORD ID | ord-4bd97bc95075499cb08dfba5100645c4 |
|---|
| Source note | uspto-grants-1997_05 |
|---|
