2-Morpholinoethylamine → HCID 86750831, compound

Participants

Reaction Steps

Following a procedure similar to that described in Example 38, but using 100 mg (0.137 mmol) of 1-{(2S,3S)-3-[N2 -(4-bromoacetamidophenoxy)acetyl-L-asparaginyl]amino-2-hydroxy-4-phenylbutyryl}-N-t-butyl-L-prolinamide and 1 ml of 4-(2-aminoethyl)morpholine, 17 mg of the title compound were obtained as a colorless powder, melting at 123°-132° C.

Provenance & Evidence