HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19047729, compound → Methyl 3-amino-4-ethylbenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19047729 | HCID 19047729 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Hydrate;hydrochloride | HCID 21885828 | — |
| Product | Methyl 3-amino-4-ethylbenzoate | HCID 13399999 | — |
Reaction Steps
The method described in Step 2. of Example 1 was applied to a solution of 35 (0.17 g) in methanol (20 mL) and 10% hydrochloric acid/water (5 mL) to prepare the above named compound. NMR (300 MHz, CDCl3) δ 7.40 (1H, d, J=8 Hz), 7.34 (1H, s), 7.10 (1H, d, J=8 Hz), 3.88 (3H, s), 3.71 (2H, b), 2.54 (2H, q, J=8 Hz), 1.26 (3H, t, J=8 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05631280 |
| Source dataset | uspto-grants-1997_05 |
| ORD ID | ord-2e9ad006c0b44d42b5792a0cee082fac |
| Source note | uspto-grants-1997_05 |